Crystal structure of (1Z,2E)-cinnamaldehyde oxime
نویسندگان
چکیده
منابع مشابه
Crystal structure of (1Z,2E)-cinnamaldehyde oxime
The title compound, C9H9NO, crystallized with two independent mol-ecules (A and B) in the asymmetric unit. The conformation of the two mol-ecules differs slightly with the phenyl ring in mol-ecule A, forming a dihedral angle of 15.38 (12)° with the oxime group (O-N=C), compared to the corresponding angle of 26.29 (11)° in mol-ecule B. In the crystal, the A and B mol-ecules are linked head-to-he...
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The title compound, C14H13NO2, is a commercially available material and can be used as a multidentate ligand. The mol-ecule of the asymmetric unit has an R configuration, while the corresponding S-configured mol-ecule of the racemic mixture is generated by a crystallographic centre of symmetry. Both hy-droxy groups (the H atom of the oxime group is equally disordered over two positions) are inv...
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The title compound, C10H8BrNO2, is almost planar (r.m.s. deviation for the non-H atoms = 0.031 Å) and the conformation across the C=N bond is trans. Further, the O atom of the benzo-furan ring is syn to the N atom of the oxime group. In the crystal, inversion dimers linked by pairs of O-H⋯N hydrogen bonds generate R 2 (2)(6) loops. Very weak aromatic π-π stacking inter-actions [centroid-centroi...
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The first crystal structure of a phenylcyanamide cobaltoxime (cobaloxime) complex is reported. This compound is trans-[Co((DO)(DOH)pn)(2,5-Cl2pcyd)2], and consits of an imine-oxime equatorial ligand ((DO)(DOH)pn) and two 2,5-dichlorophenylcyanamide ligands in axial positions. Crystals of trans- [Co((DO)(DOH)pn)(2,5-Cl2pcyd)2] were grown by ether diffusion into an acetonitrile solution of the co...
متن کاملSYNTHESIS AND CRYSTAL STRUCTURE OF [PPh ] [WOS (CUNCS) ]
The reaction of [PPhJ, NOS,] with CuCl and KSCN (1 :3:3) in acetone produces the yell-ow crystals of [PPh,], [WOS,(CuNCS),]. The crystals are triclinic, space group P1(2), z=2, a=12.4823(7), b=12.9224(7), c=18.6395(10)?, ?=83.907(5), ?= 73.152(4), Y= 65.194(4)'. The crystal structure was determined by single crystal Xray diffraction methods (Mo-K ?) and refined by least-squares calculations ...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Crystallographic Communications
سال: 2015
ISSN: 2056-9890
DOI: 10.1107/s2056989015023853